KFU. Card publication. Synthesis of 1-phenyl-3-(quinolin-8-ylamino)prop-2-en-1-one and analysis of its structure by X-ray crystallography, NMR, UV-Vis spectroscopy and DFT calculations

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SYNTHESIS OF 1-PHENYL-3-(QUINOLIN-8-YLAMINO)PROP-2-EN-1-ONE AND ANALYSIS OF ITS STRUCTURE BY X-RAY CRYSTALLOGRAPHY, NMR, UV-VIS SPECTROSCOPY AND DFT CALCULATIONS

Form of presentation

Articles in international journals and collections

Year of publication

2024

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Authors, employees of KFU

Savostina Lyudmila Ivanovna, author

Turanov Aleksandr Nikolaevich, author

Turanova Olga Alekseevna, author

Sharipova Alsu Rinatovna, author

Other authors

Volkov Mikhail Yurevich, author

Gubaydullin Aydar Timergalievich, author

Authors, postgraduates KFU

Shaydullina Amina Firdusovna, postgraduate kfu

Bibliographic description in the original language

Volkov M.Yu. Synthesis of 1-phenyl-3-(quinolin-8-ylamino)prop-2-en-1-one and analysis of its structure by X-ray crystallography, NMR, UV-Vis spectroscopy and DFT calculations / M.Yu. Volkov, A.R. Sharipova, O.A. Turanova, A.T. Gubaidullin, A.F. Shaidullina, L.I. Savostina, A.N. Turanov // ChemistrySelect. – 2024. – V. 9, � 8. – P. e202304190. https://doi.org/10.1002/slct.202304190

Annotation

1-phenyl-3-(quinolin-8-ylamino)prop-2-en-1-one was obtained by a two-step synthesis. From X-ray crystallography, NMR and UV-vis spectra it follows that in the crystalline state and in solutions, regardless of the polarity of the solvent, 1-phenyl-3-(quinolin-8-ylamino)prop-2-en-1-one exists in the ketone form of the cis-isomer. DFT calculations confirmed that the cis-isomer is the most energetically favorable among all its isomers.

Keywords

NMR, UV, DFT

The name of the journal

CHEMISTRYSELECT

Please use this ID to quote from or refer to the card

https://repository.kpfu.ru/eng/?p_id=303143&p_lang=2

Resource files

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ChemistrySelect_2024.pdf	1,98	pdf	show / download

Full metadata record

Field DC	Value	Language
dc.contributor.author	Savostina Lyudmila Ivanovna	ru_RU
dc.contributor.author	Turanov Aleksandr Nikolaevich	ru_RU
dc.contributor.author	Turanova Olga Alekseevna	ru_RU
dc.contributor.author	Sharipova Alsu Rinatovna	ru_RU
dc.contributor.author	Volkov Mikhail Yurevich	ru_RU
dc.contributor.author	Gubaydullin Aydar Timergalievich	ru_RU
dc.contributor.author	Shaydullina Amina Firdusovna	ru_RU
dc.contributor.author	Shaydullina Amina Firdusovna	ru_RU
dc.date.accessioned	2024-01-01T00:00:00Z	ru_RU
dc.date.available	2024-01-01T00:00:00Z	ru_RU
dc.date.issued	2024	ru_RU
dc.identifier.citation	Volkov M.Yu. Synthesis of 1-phenyl-3-(quinolin-8-ylamino)prop-2-en-1-one and analysis of its structure by X-ray crystallography, NMR, UV-Vis spectroscopy and DFT calculations / M.Yu. Volkov, A.R. Sharipova, O.A. Turanova, A.T. Gubaidullin, A.F. Shaidullina, L.I. Savostina, A.N. Turanov // ChemistrySelect. – 2024. – V. 9, � 8. – P. e202304190. https://doi.org/10.1002/slct.202304190	ru_RU
dc.identifier.uri	https://repository.kpfu.ru/eng/?p_id=303143&p_lang=2	ru_RU
dc.description.abstract	CHEMISTRYSELECT	ru_RU
dc.description.abstract	1-phenyl-3-(quinolin-8-ylamino)prop-2-en-1-one was obtained by a two-step synthesis. From X-ray crystallography, NMR and UV-vis spectra it follows that in the crystalline state and in solutions, regardless of the polarity of the solvent, 1-phenyl-3-(quinolin-8-ylamino)prop-2-en-1-one exists in the ketone form of the cis-isomer. DFT calculations confirmed that the cis-isomer is the most energetically favorable among all its isomers.	ru_RU
dc.language.iso	ru	ru_RU
dc.subject	NMR	ru_RU
dc.subject	UV	ru_RU
dc.subject	DFT	ru_RU
dc.title	Synthesis of 1-phenyl-3-(quinolin-8-ylamino)prop-2-en-1-one and analysis of its structure by X-ray crystallography, NMR, UV-Vis spectroscopy and DFT calculations	ru_RU
dc.type	Articles in international journals and collections	ru_RU