KFU. Card publication. Triphenylphosphine in reactions with ?-haloalkylcarboxylic acids

KAZAN
FEDERAL UNIVERSITY

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TRIPHENYLPHOSPHINE IN REACTIONS WITH ?-HALOALKYLCARBOXYLIC ACIDS

Form of presentation

Articles in international journals and collections

Year of publication

2016

Язык

английский

Authors, employees of KFU

Aksunova Alfiya Faritovna, author

Bakhtiyarova Yuliya Valerevna, author

Galkin Vladimir Ivanovich, author

Galkina Irina Vasilevna, author

Gnezdilov Oleg Ivanovich, author

Islamov Daut Rinatovich, author

Romanov Semen Romanovich, author

Authors, postgraduates KFU

Aksunova Alfiya Faritovna, postgraduate kfu

Romanov Semyon Romanovich, postgraduate kfu

Bibliographic description in the original language

Romanov, S.R. Triphenylphosphine in Reactions with ω-Haloalkylcarboxylic Acids/ S.R. Romanov, A.F. Aksunova, D.R. Islamov, A.B. Dobrynin, D.B. Krivolapov, O.N. Kataeva, Y.V. Bakhtiyarova, O.I. Gnezdilov, I.V. Galkina,V.I. Galkin// Phosphorus, Sulfur, and Silicon and the Related Elements. ? 2016. ? V.191. ? N.11-12. ? P.1637-1639

Annotation

Stable phosphonium salts were synthesized by the phosphorylation of a series of ω- haloalkylcarboxylic acids with triphenylphosphine. In a second step the resulting phosphonium salts have been treated with 1 М aqueous solution of sodium hydroxide to form the corresponding carboxylate phosphabetaines. The structure of the isolated compounds was determined by IR and NMR spectroscopy, elemental analysis and X-ray crystallographic studies. Their thermal stability was studied by simultaneous thermogravimetry and differential scanning calorimetry.

Keywords

phosphonium salts, synthes, phosphorylation, IR spectroscopy, NMR spectroscopy, elemental analysis, X-ray analysis

The name of the journal

Phosphorus, Sulfur and Silicon and the Related Elements

URL

https://www.scopus.com/inward/record.uri?eid=2-s2.0-84992612593&partnerID=40&md5=6aacf8536f70995f3168585ec13fc932

Please use this ID to quote from or refer to the card

https://repository.kpfu.ru/eng/?p_id=147427&p_lang=2

Full metadata record

Field DC	Value	Language
dc.contributor.author	Aksunova Alfiya Faritovna	ru_RU
dc.contributor.author	Bakhtiyarova Yuliya Valerevna	ru_RU
dc.contributor.author	Galkin Vladimir Ivanovich	ru_RU
dc.contributor.author	Galkina Irina Vasilevna	ru_RU
dc.contributor.author	Gnezdilov Oleg Ivanovich	ru_RU
dc.contributor.author	Islamov Daut Rinatovich	ru_RU
dc.contributor.author	Romanov Semen Romanovich	ru_RU
dc.contributor.author	Aksunova Alfiya Faritovna	ru_RU
dc.contributor.author	Romanov Semyon Romanovich	ru_RU
dc.date.accessioned	2016-01-01T00:00:00Z	ru_RU
dc.date.available	2016-01-01T00:00:00Z	ru_RU
dc.date.issued	2016	ru_RU
dc.identifier.citation	Romanov, S.R. Triphenylphosphine in Reactions with ω-Haloalkylcarboxylic Acids/ S.R. Romanov, A.F. Aksunova, D.R. Islamov, A.B. Dobrynin, D.B. Krivolapov, O.N. Kataeva, Y.V. Bakhtiyarova, O.I. Gnezdilov, I.V. Galkina,V.I. Galkin// Phosphorus, Sulfur, and Silicon and the Related Elements. ? 2016. ? V.191. ? N.11-12. ? P.1637-1639	ru_RU
dc.identifier.uri	https://repository.kpfu.ru/eng/?p_id=147427&p_lang=2	ru_RU
dc.description.abstract	Phosphorus, Sulfur and Silicon and the Related Elements	ru_RU
dc.description.abstract	Stable phosphonium salts were synthesized by the phosphorylation of a series of ω- haloalkylcarboxylic acids with triphenylphosphine. In a second step the resulting phosphonium salts have been treated with 1 М aqueous solution of sodium hydroxide to form the corresponding carboxylate phosphabetaines. The structure of the isolated compounds was determined by IR and NMR spectroscopy, elemental analysis and X-ray crystallographic studies. Their thermal stability was studied by simultaneous thermogravimetry and differential scanning calorimetry.	ru_RU
dc.language.iso	ru	ru_RU
dc.subject	phosphonium salts	ru_RU
dc.subject	synthes	ru_RU
dc.subject	phosphorylation	ru_RU
dc.subject	IR spectroscopy	ru_RU
dc.subject	NMR spectroscopy	ru_RU
dc.subject	elemental analysis	ru_RU
dc.subject	X-ray analysis	ru_RU
dc.title	Triphenylphosphine in reactions with ?-haloalkylcarboxylic acids	ru_RU
dc.type	Articles in international journals and collections	ru_RU